External Circulation Heating Technology

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External Circulation Heating Technology

Glycerol distillation clean production technology (based on external circulation heating distillation technology)

The company specializes in providing engineering amplification and information solutions for chemical companies. Acting as a bachelorarbeit hilfe for industrial solutions, the business involves chemical engineering to expand design, data management, automation and many other aspects. The technical team is the core competency of our company. The company’s products have the following series:

3D rapid design solution for chemical plants (professional chemical design team, with special emphasis on small-scale industrialization of technology research)

Our advantages in the glycerol Technology Series

The production capacity of internal heating distillation equipment is 10 -100T / D.
The production capacity of the external circulation distillation equipment is 50 -300T / D,
997 high gauge glycerol distillation process production line.
Clean transformation technology of traditional distillation production line.
Clean production technology of complex glycerol, such as sulphate.
Continuous decolorization technology

Comparison of internal and external heating distillation technology

Type	Distillation Temperature	Vacuum Degree	Capacity	Yield	Glycerol treatment	Product quality
Type	Distillation Temperature	(Kpa)	（T/D）	Yield	Glycerol treatment	Product quality
Internal coil heating	180~210	6~8	10~100	Low	OK	Low
External circulation heating	150~170	0.2~0.3	50~300	High	Not recommended	High

The advantages of external circulation heating glycerol technology are:

The technology of external circulation and low energy consumption is equal to the existing technology.
The treatment temperature is below 160 degrees, which greatly reduces the generation of decomposition and polymerization.
The circulating cooling water is not contacted with the system, and it will never pollute.
Glycerol residues from non glycerol organic matter and polyglycerol are sold as industrial auxiliaries after desalting.
The salt in raw material is on-line continuous separation technology, which is mainly removed in solid form, and it can be sold as industrial salt.
Environmental design also achieves excellent level. The whole system is designed with negative pressure, without any sensitive gas leakage. At the same time, the sewage produced by the system is minimized and completely cleaned, sent to the sewage treatment center to deal with the discharge of the standard.
The water circulation pump adopts the technology of circulating closed water, which greatly saves the fresh water consumption.
Energy recycling is maximized, and processing cost is highly competitive.
A full set of DCS designs, continuous import and export, smooth operation, excellent quality and minimum labor force.
The circulating cooling water is not contacted with the system, and it will never pollute.
The yield of distillation is 2-3 percentage points higher than that of traditional process.
80% of the finished products were obtained with a high content of 99.9

Necessary basic public utilities:

Heat conduction oil furnace 600 thousand kcal / tons of finished products.
Cooling water 60 cubic / ton finished product.
Electric 10KW / ton finished product.

Separation Purpose

Process schematic

Three wastes treatment scheme:

Salt free waste water (to be treated at the sewage station).

Distillation section: 500 tons (COD: 4, 000 ppm).

Solid

Solid salt (sold as industrial salt) (containing a small amount of M, O, N, G, polyglycerol, glycerol): 50~80 kg.

Activated carbon (activated carbon plant recovery) (containing glycerin): 3~8 times.

Polyglycerol residue (as a sale of industrial auxiliaries).

Distillation section: 50~80 tons

Processing cost

Because of the difference in quality of crude glycerol, the yield fluctuating range is between 90 and 98%, and generally reaches 95%.

(Calculated with 1000KG finished products):

Factory scene

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